Chemical Analysis

Bruker ELEXSYS E580 and E780 EPR Systems

The E780 is a 263 GHz (high frequency) EPR spectrometer which represents a cutting-edge turn-key technology for Electron Spin Resonance spectroscopy. Additionally, E580 is equipped with a rapid scan attachment that allows a 10µs resolution of time lapse experiments and observation of changes in paramagnetic centers during reactions and live processes.

Both system provide capabilities of both pulse and continuous wave measurements. This allows for ESEEM, Pulse-ENDOR, Pulse-ELDOR DEER and HYSCORE for application in Life science, Material science and Quantum computing.

  • 9.8 GHz (E580) and 263 GHz (E780) operation frequency
  • Quasi optical front end
  • Reflection and induction mode
  • CW and Pulse operation
  • Single mode resonator
  • Non-resonant probe
  • Sample temperature: 4 - 300 K (Stinger and High Temp. attachment)
  • Superconducting magnet (E780)

Bruker ELEXSYS E580 and E780 Electron Spin Resonance (EPR) SystemBruker ELEXSYS E580 and E780 Electron Spin Resonance (EPR) System in LSU Chemistry Building, 301 Choppin Hall

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Renishaw inVia Reflex Raman Spectroscope

Renishaw inVia Reflex Raman Microscope enables chemical identification of elements and compounds with a spatial resolution of ~1 µm.

Raman shifts within 150 cm-1 of the excitation frequency can be measured at excitation wavelengths of either 532 nm,  633 nm, or 785 nm, with a spectral resolution of ~1 cm-1.

Objectives: 5x, 20x, 50x, 50x (long-working distance), and 100x.

Its features include the following:

  • Stereo viewing, memorized and automatic post collection viewing and combined white light and laser video viewing
  • Software microscope control
  • Automatic white light/Raman switching and white light saving with data
  • White light auto-focus (LiveTrack)

  • Automated measurement queuing
  • Automatic focus tracking (LiveTrack)

  • Internal neon wavelength calibration source
  • Internal reference standards for auto-calibration
  • Automated Raman calibration correction and performance health check
  • Laser auto-align and Raman signal auto-align

Renishaw inVia Reflex Raman SpectroscopeRenishaw inVia Reflex Raman Spectroscope in Chemistry & Materials Building, Room 168.

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Energy-dispersive X-ray Spectroscopy

There are two EDS detectors currently at AMAC—the EDAX Apollo XL EDS detector integrated with the FEI Quanta 3D FEG GaFIBSEM Dual Beam System and the Oxford UltiMax65 EDS detector integrated with the ThermoFisher Helio G5 CXe PFIBSEM dual Beam System.

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